TA Instruments

AR1755-0004f

15/03/2013 14:38:57

Sample name	ASW Blank coupon#20 + DI + beads 
Sample notes	 
Experiment notes	DI Deionised water, 25 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1755
Run number	4 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 14:38:57

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	No
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	No

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 100.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	No

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	0.4094 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	2
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.14 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0080	99.99	84.770	10000	20.0	0.1507	1.008	27.63	125.0	0.2211	614.2	104.1650	0.03932	130.21	13021	3.411E-3	0.0	0.0
2.0040	99.99	112.24	10000	20.0	0.1473	2.004	36.59	125.0	0.2927	600.2	191.8550	0.03841	239.82	23982	3.411E-3	0.0	0.0
3.0080	100.0	113.08	10000	20.0	0.1438	3.008	36.86	125.0	0.2949	586.1	279.6640	0.03751	349.58	34958	3.411E-3	0.1	0.1
4.0040	100.0	111.70	10000	20.0	0.1465	4.004	36.41	125.0	0.2913	596.8	367.1950	0.03820	458.99	45899	3.411E-3	0.1	0.1
5.0040	100.0	111.95	10000	20.0	0.1489	5.004	36.49	125.0	0.2919	606.8	499.1180	0.03883	623.90	62390	3.411E-3	0.1	0.1
6.0080	100.0	112.36	10000	20.0	0.1491	6.008	36.62	125.0	0.2930	607.6	587.0390	0.03889	733.80	73380	3.411E-3	0.1	0.1
7.0120	100.0	111.66	10000	20.0	0.1469	7.012	36.40	125.0	0.2912	598.5	675.1360	0.03830	843.92	84392	3.411E-3	0.1	0.1
8.0040	100.0	111.32	10000	20.0	0.1457	8.004	36.29	125.0	0.2903	593.5	763.0200	0.03799	953.78	95378	3.411E-3	0.1	0.1
9.0040	100.0	111.71	10000	20.0	0.1479	9.004	36.41	125.0	0.2913	602.6	896.8000	0.03857	1121.0	1.1210E5	3.411E-3	0.2	0.2
10.008	100.0	111.25	10000	20.0	0.1453	10.008	36.26	125.0	0.2901	591.9	982.8990	0.03788	1228.6	1.2286E5	3.411E-3	0.2	0.2
11.004	100.0	110.48	10000	20.0	0.1469	11.004	36.01	125.0	0.2881	598.5	1072.0400	0.03830	1340.1	1.3401E5	3.411E-3	0.2	0.2
12.008	100.0	111.33	10000	20.0	0.1441	12.008	36.29	125.0	0.2903	586.9	1203.4000	0.03756	1504.3	1.5043E5	3.411E-3	0.2	0.2
13.024	100.0	111.23	10000	20.0	0.1471	13.024	36.26	125.0	0.2900	599.3	1295.3199	0.03836	1619.2	1.6192E5	3.411E-3	0.2	0.2
14.020	100.0	110.74	10000	20.0	0.1453	14.020	36.10	125.0	0.2888	591.9	1379.9800	0.03788	1725.0	1.7250E5	3.411E-3	0.2	0.2
15.020	100.0	111.28	10000	20.0	0.1471	15.020	36.27	125.0	0.2902	599.3	1466.7100	0.03836	1833.4	1.8334E5	3.411E-3	0.3	0.3
16.020	100.0	111.31	10000	20.0	0.1441	16.020	36.28	125.0	0.2903	586.9	1598.9000	0.03756	1998.6	1.9986E5	3.411E-3	0.3	0.3
17.004	100.0	110.18	10000	20.0	0.1469	17.004	35.91	125.0	0.2873	598.5	1687.0300	0.03830	2108.8	2.1088E5	3.411E-3	0.3	0.3
18.024	100.0	109.81	10000	20.0	0.1451	18.024	35.79	125.0	0.2863	591.1	1775.0000	0.03783	2218.8	2.2188E5	3.411E-3	0.3	0.3
19.064	100.0	110.93	10000	20.0	0.1479	19.064	36.16	125.0	0.2893	602.6	1906.5300	0.03857	2383.2	2.3832E5	3.411E-3	0.3	0.3
20.020	100.0	110.57	10000	20.0	0.1453	20.020	36.04	125.0	0.2883	591.9	1995.3700	0.03788	2494.2	2.4942E5	3.411E-3	0.3	0.3
21.020	100.0	109.87	10000	20.0	0.1483	21.020	35.81	125.0	0.2865	604.3	2083.1499	0.03867	2603.9	2.6039E5	3.411E-3	0.4	0.4
22.008	100.0	110.60	10000	20.0	0.1451	22.008	36.05	125.0	0.2884	591.1	2170.5701	0.03783	2713.2	2.7132E5	3.411E-3	0.4	0.4
23.048	100.0	109.81	10000	20.0	0.1447	23.048	35.79	125.0	0.2863	589.4	2302.3000	0.03772	2877.9	2.8779E5	3.411E-3	0.4	0.4
24.004	100.0	108.51	10000	20.0	0.1453	24.004	35.37	125.0	0.2829	591.9	2390.3201	0.03788	2987.9	2.9879E5	3.411E-3	0.4	0.4
25.024	100.0	109.01	10000	20.0	0.1473	25.024	35.53	125.0	0.2843	600.2	2478.8201	0.03841	3098.5	3.0985E5	3.411E-3	0.4	0.4
26.024	100.0	108.17	10000	20.0	0.1471	26.024	35.26	125.0	0.2820	599.3	2566.2300	0.03836	3207.8	3.2078E5	3.411E-3	0.4	0.4
27.004	100.0	108.04	10000	20.0	0.1465	27.004	35.22	125.0	0.2817	596.8	2698.2300	0.03820	3372.8	3.3728E5	3.411E-3	0.5	0.5
28.004	100.0	110.55	10000	20.0	0.1451	28.004	36.03	125.0	0.2883	591.1	2786.1399	0.03783	3482.7	3.4827E5	3.411E-3	0.5	0.5
29.008	100.0	108.39	10000	20.0	0.1451	29.008	35.33	125.0	0.2826	591.1	2874.1299	0.03783	3592.7	3.5927E5	3.411E-3	0.5	0.5
30.008	100.0	110.62	10000	20.0	0.1483	30.008	36.05	125.0	0.2884	604.3	2962.0500	0.03868	3702.6	3.7026E5	3.411E-3	0.5	0.5
31.020	100.0	110.46	10000	20.0	0.1477	31.020	36.01	125.0	0.2880	601.8	3094.0100	0.03851	3867.5	3.8675E5	3.411E-3	0.5	0.5
32.004	100.0	109.45	10000	20.0	0.1471	32.004	35.67	125.0	0.2854	599.3	3182.3000	0.03836	3977.9	3.9779E5	3.411E-3	0.5	0.5
33.004	100.0	109.68	10000	20.0	0.1453	33.004	35.75	125.0	0.2860	591.9	3269.8601	0.03788	4087.3	4.0873E5	3.411E-3	0.6	0.6
34.004	100.0	110.43	10000	20.0	0.1455	34.004	35.99	125.0	0.2880	592.7	3402.2800	0.03793	4252.9	4.2529E5	3.411E-3	0.6	0.6
35.004	100.0	108.87	10000	20.0	0.1461	35.004	35.48	125.0	0.2839	595.2	3489.8201	0.03809	4362.3	4.3623E5	3.411E-3	0.6	0.6
36.092	100.0	110.98	10000	20.0	0.1438	36.092	36.18	125.0	0.2894	586.1	3577.7900	0.03751	4472.2	4.4722E5	3.411E-3	0.6	0.6
37.004	100.0	111.43	10000	20.0	0.1459	37.004	36.32	125.0	0.2906	594.4	3665.7700	0.03804	4582.2	4.5822E5	3.411E-3	0.6	0.6
38.008	100.0	109.69	10000	20.0	0.1461	38.008	35.75	125.0	0.2860	595.2	3798.0701	0.03809	4747.6	4.7476E5	3.411E-3	0.6	0.6
39.004	100.0	108.85	10000	20.0	0.1441	39.004	35.48	125.0	0.2839	586.9	3885.6599	0.03757	4857.1	4.8571E5	3.411E-3	0.7	0.7
40.004	100.0	109.71	10000	20.0	0.1465	40.004	35.76	125.0	0.2861	596.8	3973.5701	0.03820	4967.0	4.9670E5	3.411E-3	0.7	0.7
41.004	100.0	110.90	10000	20.0	0.1459	41.004	36.15	125.0	0.2892	594.4	4062.1201	0.03804	5077.7	5.0777E5	3.411E-3	0.7	0.7
42.040	100.0	110.10	10000	20.0	0.1469	42.040	35.89	125.0	0.2871	598.5	4193.9702	0.03830	5242.5	5.2425E5	3.411E-3	0.7	0.7
43.004	100.0	111.17	10000	20.0	0.1459	43.004	36.23	125.0	0.2899	594.4	4281.4800	0.03804	5351.9	5.3519E5	3.411E-3	0.7	0.7
44.036	100.0	109.97	10000	20.0	0.1449	44.036	35.84	125.0	0.2868	590.2	4371.3799	0.03777	5464.2	5.4642E5	3.411E-3	0.7	0.7
45.004	100.0	111.33	10000	20.0	0.1505	45.004	36.29	125.0	0.2903	613.4	4501.3901	0.03926	5626.7	5.6267E5	3.411E-3	0.8	0.8
46.020	100.0	109.38	10000	20.0	0.1477	46.020	35.65	125.0	0.2852	601.8	4590.0898	0.03851	5737.6	5.7376E5	3.411E-3	0.8	0.8
47.020	100.0	109.65	10000	20.0	0.1451	47.020	35.74	125.0	0.2859	591.1	4677.4702	0.03783	5846.8	5.8468E5	3.411E-3	0.8	0.8
48.004	100.0	110.71	10000	20.0	0.1491	48.004	36.09	125.0	0.2887	607.6	4769.2700	0.03888	5961.6	5.9616E5	3.411E-3	0.8	0.8
49.004	100.0	109.12	10000	20.0	0.1473	49.004	35.57	125.0	0.2845	600.2	4897.1499	0.03841	6121.4	6.1214E5	3.411E-3	0.8	0.8
50.004	100.0	110.10	10000	20.0	0.1461	50.004	35.89	125.0	0.2871	595.2	4985.1602	0.03809	6231.5	6.2315E5	3.411E-3	0.8	0.8
51.008	100.0	109.58	10000	20.0	0.1461	51.008	35.72	125.0	0.2857	595.2	5073.1001	0.03809	6341.4	6.3414E5	3.411E-3	0.9	0.9
52.008	100.0	110.06	10000	20.0	0.1469	52.008	35.88	125.0	0.2870	598.5	5161.0698	0.03831	6451.3	6.4513E5	3.411E-3	0.9	0.9
53.000	100.0	110.62	10000	20.0	0.1461	53.000	36.06	125.0	0.2884	595.2	5293.4302	0.03809	6616.8	6.6168E5	3.411E-3	0.9	0.9
54.008	100.0	109.15	10000	20.0	0.1457	54.008	35.58	125.0	0.2846	593.5	5380.9902	0.03799	6726.2	6.7262E5	3.411E-3	0.9	0.9
55.020	100.0	108.71	10000	20.0	0.1441	55.020	35.44	125.0	0.2835	586.9	5468.8999	0.03756	6836.1	6.8361E5	3.411E-3	0.9	0.9
56.008	100.0	108.76	10000	20.0	0.1449	56.008	35.45	125.0	0.2836	590.2	5601.3599	0.03777	7001.7	7.0017E5	3.411E-3	0.9	0.9
57.004	100.0	109.98	10000	20.0	0.1457	57.004	35.85	125.0	0.2868	593.5	5689.2500	0.03799	7111.6	7.1116E5	3.411E-3	1.0	1.0
58.004	100.0	111.75	10000	20.0	0.1449	58.004	36.43	125.0	0.2914	590.2	5777.3901	0.03777	7221.7	7.2217E5	3.411E-3	1.0	1.0
59.004	100.0	109.95	10000	20.0	0.1441	59.004	35.84	125.0	0.2867	586.9	5864.8101	0.03756	7331.0	7.3310E5	3.411E-3	1.0	1.0
60.004	100.0	110.44	10000	20.0	0.1461	60.004	36.00	125.0	0.2880	595.2	5996.7402	0.03809	7495.9	7.4959E5	3.411E-3	1.0	1.0

